CAVIAR: ROE PROCESSING MANUAL  

FOREWORD

1.0 CAVIAR PRODUCTS
1.1 INTRODUCTION
1.2 THE WORD 'CAVIAR'
1.3 LABELLING PRODUCTS
1.4 CANADIAN ROE RESOURCES
2.0 ROE
2.1 OVARIES
2.2 MATURITY
2.3 YIELD
2.4 FROZEN ROE
2.5 GRADING FRESHNESS
2.6 CHEMICAL COMPOSITION
2.7 EGG STRUCTURE
3.0 SCREENING
3.1 SCREENING OPERATION
3.2 SCREENING TECHNIQUE
3.3 SCREENING DEVICES
3.4 MECHANIZED SCREENING
4.0 SALTING
4.1 PRESERVATIVE ACTION
4.2 THE SALTING MECHANISM
4.3 SALINITY
4.5 CURING EFFECT
4.6 SALTING TIME
4.7 SALINITY MEASUREMENTS
4.8 DRAINING, EGG VISCOSITY AND VISCOSITY MEASUREMENTS
5.0 PACKING
5.1 FREEZING AND REFRIGERATION
5.2 BULK AND RETAIL PACKAGE
5.3 PACKAGE TYPE
5.4 CHEMICAL PRESERVATION
5.5 ADDITIVES AND DYES
5.6 PASTEURIZATION
5.7 PACKAGING OVERVIEW
6.0 QUALITY AND SHELF-LIFE
6.1 QUALITY GRADING
6.2 ORGANOLEPTIC TRIALS
6.3 DEFECTS
6.4 CHEMICAL AND BACTERIOLOGICAL EXAMINATIONS
6.5 SHELF-LIFE
6.6 QUALITY CONTROL AND ASSURANCE
7.0 THE CAVIAR SHOP
7.1 LAYOUT AND MECHANIZATION
7.2 PLANNING A SALMON CAVIAR OPERATION
7.3 WATER QUALITY
7.4 SALT QUALITY
7.5 BRINE PROPERTIES
7.6 BRINE MAKING REQUIREMENTS AND APPARATUS
7.7 SALTING TANKS
7.8 MISCELLANEOUS TOOLS, INSTRUMENTS AND MECHANISMS
7.9 SANITATION
8.0 PROCESSING DIFFERENT SPECIES
8.1 HARVESTING LUMPFISH ROE
8.2 PROCESSING LUMPFISH CAVIAR
8.3 WHITEFISH AND OTHER ORDINARY FISH
8.4 STURGEON FISHERIES
8.5 PROCESSING STURGEON CAVIAR
8.6 SALMON FISHERIES
8.7 PROCESSING SALMON CAVIAR
8.8 ARTIFICIAL CAVIARS

8.0 PROCESSING DIFFERENT SPECIES

8.7 PROCESSING SALMON CAVIAR

The technological steps involved in salmon caviar production were discussed in previ-ous chapters. This chapter offers a condensed summary of processing granular salmon caviar.

Salmon caviar is marketed as fresh (non-pasteurized), pasteurized and chemically pre-served for both frozen and chilled storage, see Figure 8-14. Smoking or artificial en-hancement of salmon caviar colour or flavour is not popular. The steps involved in proc-essing salmon caviar are given on Figure 8-13. Salmon caviar is processed predominantly from fresh Chum and in part from Pink and other salmon ovaries at the right maturity stage.

FIGURE 8-13

SALMON CAVIAR PROCESSING

After catch the fish is kept on ice or in refrigerated sea water not longer than 48 hours. The fish are delivered right to the processing site and ovaries are extracted and processed without delay. Fresh and live fish are bled before the ovaries are extracted. Manual cut-ting and ovary extraction is preferable to machine butchering, because the essentially sterile ovaries can be carefully detached before total cleaning of the belly cavity which may cause cross contamination. Manual butchering ensures minimal contamination. Care must be taken not to cut into the ovaries when splitting the belly, because it is difficult to get rid of the broken egg membranes during the subsequent technological steps.

If there is any delay (even for two hours) in processing, the extracted eggs should be placed in cold storage. Ovaries are graded mainly by freshness, because fish delivered from the same area are usually of the same maturity. Ovaries are considered Grade No. 1 when they are fully developed, firm, elastic, odourless, shiny and bright orange or or-ange-red in colour. Sometimes one can observe local darkening of colour of the posterior ovary tip or on the parts adjacent to the backbone. If the darkening is not intensive the darker parts are torn off and the ovaries still qualify for Grade No. 1. Vessels located along the ovaries and filled with blood and pieces of kidney do not discriminate against the ovaries being Grade No. 1. While screening, the blood, blood clots or kidney pieces will drain off or be caught by the slope screen. It is not recommended to use knives. Torn ovaries, which have lost their intact shape because of rough handling could also be con-sidered Grade No. 1 if this is the only defect. As ovaries get darker in colour, soft, slimy and less elastic they are graded out for No. 2 caviar or to be used for other than caviar products, e.g. sujiko, bait. Failure to grade before screening contributes to cross contami-nation, makes cleaning from membranes more difficult and generally down grades the whole lot. Graded ovaries are quickly rinsed and drained with ice cold water or light brine. Rinsing can be done by dipping perforated baskets, partially filled with ovaries, into a vessel with running cold water, which is constantly decanted to get rid of impuri-ties. The use of ice cold water (1 to +5°C) strengthens the membranes and makes screen-ing more efficient. If ovaries are still not cold enough they are put into -2 to -3°C cold brine (15% concentration) for 2-3 minutes.

Before screening the ovaries are drained and one by one manually torn flat ('opened'). Ovaries are placed onto the first screen and rubbed through by gently pushing the ovaries into the screen and simultaneously performing circular movements with the palms of both hands. The whole surface of the screen is used. Both rubber and cotton knitted gloves are used. Soiled screens are replaced by clean ones as often as needed, usually every 1 to 2 hours. Soiled screens are washed free of debris in a specially designated area using high pressure water jets and brushes.

The eggs run down a slope screen into a collecting basket with a mesh bottom to drain off broken egg interior liquid. It is not recommended to tap the screens in order to recover small lumps of eggs still connected to tissues and stuck in the mesh screen. These lumps are collected separate for bait processing before the screens are washed. Only eggs which freely run off the screens are introduced into the batch.

Salting is done in saturated 100% brine at temperatures of 8-12°C. Brine is prepared using salt of the highest grade. Brine is not used more than twice. The egg/brine ratio should be at least 1:3. Salt is added to the bottom of salting tanks to fortify the brine. The added salt should be of larger particle size otherwise small particles may be lifted due to agitation and stick to the eggs. This may result in oversalting.

Usually mechanical agitators are used. Manual agitation by means of a plastic paddle is used in small size operations. It is popular to tennis racquets or similar metal mesh paddles to stir the eggs manually while they are agitated in brine. This provides better mixing and also serves to remove egg lumps, broken membranes and connective tissues still remaining after screening. Netting frames, placed inside and, attached to the salting tank serve the same purpose. Salting time depends on the desired final target salinity. Usually salmon caviars are salted to 3.5 - 4.0% salinity. The salting time to achieve this salinity varies from 3 to 20 minutes. It depends on many factors e.g. mature and fresh eggs should be salted for a longer time than immature and marginally fresh ('soft') eggs. .Brine temperature and egg/brine ratio also affects salting time.

Salting can be performed in two salting sessions. For about 50% of the total salting time eggs are transferred to a tank containing clean unused brine and the salting is resumed. This makes a clean product. The second tank is then used for the next lot first salting ses-sion.

To determine what salting time is appropriate for any particular lot is impossible without experimenting with small size batches which model the actual conditions and measure sa-linity. The salting curve i.e. salinity vs salting time, has a typical character. At the begin-ning salinity is proportional to the salting time. At the end of the process salt absorbtion slows down considerably. It is somewhere at the junction of these two phenomenon that the right salinity and the best interior yolky fluid viscosity are achieved. If the desired salinity is achieved during the period when salinity is still rising proportionally to time, watery cav-iar is produced. It may happen with immature and soft eggs. That is why lower grade salmon eggs, are held in brine longer to achieve the desired viscosity and become over-salted.

To measure salinity of one sample takes 2-3 minutes using conductometric salimeters. Dis-tilled or plain water is added to a sample in the ratio 9:1. After homogenizing and filtering (fine mesh or filter paper) the filtrate is poured through the measuring column. The elec-trodes should be kept clean and the instrument and kept rinsed after each measurement. To estimate salinity by tasting is only an additional test which aims to accumulate skill and understanding of the process. When squeezed, properly salted eggs do not release the inner liquid in the form of a jet but in the form of a honey like droplet. Other indicators of when to stop salting are: the inner fluid does not have blood colouring, and the salted dry eggs generate a rustling sound when stirred in a bowl. When eggs are

squeezed in the palm of the hand they should not lump, but should be easily detachable. Overdone eggs have a waxy mouthfeel. Agitation is stopped 10-60 seconds before the salting time is over, so that the heavier debris and broken membranes can settle to the bottom and thus they are not scooped off.

Brine may be reused if filtered and fortified to 100% saturation. Scooping is done with all kinds of plastic, metallic mesh or bamboo baskets. It is important to get the eggs out as quickly as possible. The eggs can first be put into a container and then redistributed into draining baskets. Draining is done in two steps. The first time draining lasts for a short time until the bulk of excessive brine runs off. At that time it is very convenient to candle or inspect the eggs and manually remove the remaining broken membranes using tweezers. If salted eggs contain excessive broken eggs, lumps and other impurities they could be screened through a clean screening device for a second time. Simultaneously they will get dewatered from excess brine.

When the salted egg mass is still wet it is easy to push it along the flat and sloped sur-face of the inspection table by means of wide spatulas. To make it easier to move the eggs, olive oil may be applied to the surface. If the eggs are fairly dry they are ready to be packed right away into bulk or institutional packages. If the eggs are too moist they are left for additional draining-curing for several hours. Leaving eggs overnight is widely practiced, but may result in overdrying. Draining trays or baskets are placed on shelves in a separate clean and air controlled room. Eggs are placed in layers not ex-ceeding 8-10 cm.

Mixing drained eggs with preservatives and oil can be done in low revolution shaft and drum mixers, or manually on flat metallic surfaces using spatulas. Chemical preserva-tives are diluted in minimal volumes of light brine and sprayed on the eggs in amounts to meet the regulatory restrictions for the final product, usually within 0.1%. To apply preservatives in a powder form requires thorough mixing to avoid local out-of-limit concentrations. After application, of the water soluble preservatives a mixture of a vege-table oil (e.g. olive or corn oil) and glycerol up to 0.6% can be added to prevent the eggs from sticking together and to make them look shiny. Glycerol also adds a sweetish after-taste to mask the slight natural bitterness of some eggs. The use of oils and glycerol is popular in the Soviet Union.

When caviar is packed into containers care should be taken to achieve a dense packing without air cavities. Before and during packing caviar is constantly inspected and remaining impurities are manually removed.

This is done by gently compacting the eggs layer by layer. When machine fillers are used the so called 'bottom-up' technique is used, i.e. firstly the filling nozzle discharges the product onto the container bottom and then moves up.

Bulk and institutional packages are often frozen and kept at -20°C. Second grade eggs should not be frozen to avoid excessive release of juice after thawing. Sufficient head-space should be provided to ensure successful vacuum closure. Pasteurization in a water bath at 68°-70°C for 60-90 minutes adds to product shelflife. At all times, pasteurized or not, caviar is best kept at -2 to +1°C. Washing containers after packing, and especially after vacuum packing, is mandatory to prevent microbiological build up on the container surface and around the seal.

Frozen caviar is defrosted very slowly, if possible at 2°C per day in order not to subject the eggs to the rigor of temperature changes which may result in the release of excessive juice.

Pressed salmon caviar can be made from screened immature and weak ovaries in a simi-lar way as was described for pressed sturgeon caviar. However, this product, is processed extremely rarely. Salmon caviar of different types is shown on Figure 8-14.


FIGURE 8-14: Salmonid Caviar

            a) Trout, Alaska
            b) Chum/B.C.
            c) Chum, non-pasteurized, B.C.
            d) Chum, pasteurized, B.C.